{"doi":"10.1002/jctb.280530116","title":"Synthesis of 5,5′‐Oxydimethylenebis (2‐furfural) by Thermal Dehydration of 5‐Hydroxymethyl‐2‐furfural in the Presence of Dimethylsulfoxide","abstract":"<jats:title>Abstract</jats:title><jats:p>A new method for the synthesis of 5,5′‐oxydimethylenebis (2‐furfural) by thermal dehydration of 5‐hydroxymethyl‐2‐furfural in the presence of dimethyl‐sulfoxide is described. Optimum conditions are studied by experimental design. Reaction media present a high concentration of HMF. Reaction is supposed to be rapid. Yields reach 55% with a 84% selectivity.</jats:p>","journal":"Journal of Chemical Technology &amp; Biotechnology","year":1992,"id":657419,"datarank":1.0614003114157016,"base_score":2.8903717578961645,"endowment":2.8903717578961645,"self_citation_contribution":0.4335557636844247,"citation_network_contribution":0.6278445477312767,"self_endowment_contribution":0.4335557636844247,"citer_contribution":0.6278445477312767,"corpus_percentile":null,"corpus_rank":null,"citation_count":17,"citer_count":17,"citers_with_citation_signal":16,"citers_with_endowment":16,"datacite_reuse_total":0,"is_dataset":false,"is_dataset_confidence":null,"is_data_producer":false,"deposit_databanks":null,"is_oa":false,"file_count":0,"downloads":0,"has_version_chain":false,"published_date":null,"fair_score":null,"fair_percentile":null,"algorithm_id":"datarank_citation_only_1hop_v6","ranking_scope":"data_only","authors":[{"id":1716213,"name":"Luc Rigal","orcid":null,"position":1,"is_corresponding":false},{"id":1716214,"name":"Antoine Gaset","orcid":null,"position":2,"is_corresponding":false},{"id":1716212,"name":"Christian Larousse","orcid":null,"position":0,"is_corresponding":false}],"reference_count":0,"raw_metadata":{"has_enrichment":true,"resolved":true,"title":"Synthesis of 5,5′‐Oxydimethylenebis (2‐furfural) by Thermal Dehydration of 5‐Hydroxymethyl‐2‐furfural in the Presence of Dimethylsulfoxide","abstract":"<jats:title>Abstract</jats:title><jats:p>A new method for the synthesis of 5,5′‐oxydimethylenebis (2‐furfural) by thermal dehydration of 5‐hydroxymethyl‐2‐furfural in the presence of dimethyl‐sulfoxide is described. Optimum conditions are studied by experimental design. Reaction media present a high concentration of HMF. Reaction is supposed to be rapid. Yields reach 55% with a 84% selectivity.</jats:p>","is_dataset_classified":null,"base_score":2.8903717578961645,"endowment":2.8903717578961645,"datacite_reuse_total":0,"file_count":0,"downloads":0,"views":0,"has_version_chain":false,"is_dataset":false,"is_oa":false,"pmid":"19162232","pmcid":null,"openalex_id":"https://openalex.org/W1978966661","authors":[],"funders":[],"total_grants":0,"fwci":0.0,"citation_percentile":0.04864498,"influential_citations":0,"citation_trend":[{"year":2013,"count":2},{"year":2016,"count":2},{"year":2017,"count":2},{"year":2018,"count":2},{"year":2019,"count":1},{"year":2022,"count":1},{"year":2023,"count":1},{"year":2025,"count":1},{"year":2026,"count":1}],"oa_status":"closed","license":"http://onlinelibrary.wiley.com/termsAndConditions#vor","oa_locations":[{"url":"https://api.wiley.com/onlinelibrary/tdm/v1/articles/10.1002%2Fjctb.280530116","host_type":"publisher"},{"url":"https://scijournals.onlinelibrary.wiley.com/doi/pdf/10.1002/jctb.280530116","host_type":"publisher"},{"url":"https://doi.org/10.1002/jctb.280530116","host_type":"journal"}],"fields_of_study":["Chemical Synthesis and Reactions","Carbohydrate Chemistry and Synthesis","Multicomponent Synthesis of Heterocycles"],"mesh_terms":[],"keywords":["Furfural","Hydroxymethyl","Dehydration","Chemistry","Selectivity","Dimethyl sulfoxide","Organic chemistry","Dehydration reaction","Catalysis","Biochemistry"],"sdg_mappings":[{"sdg_number":0,"sdg_label":"Clean water and sanitation"}],"linked_datasets":[],"clinical_trials":[],"software_tools":[],"database_accessions":[],"source":"live","citation_network_status":"fetched"},"created_at":"2026-08-12T01:02:02.622292Z","pmid":null,"pmcid":null,"fwci":null,"citation_percentile":null,"influential_citations":0,"oa_status":null,"license":null,"views":0,"total_file_size_bytes":0,"version_count":0,"fair_f":null,"fair_a":null,"fair_i":null,"fair_r":null,"fair_zscore":null,"fair_rationale":null,"fair_model":null,"fair_agent_version":null,"fair_fulltext_source":null,"fair_has_llm":null,"fair_computed_at":null,"clinical_trials":[],"software_tools":[],"db_accessions":[],"linked_datasets":[],"topics":[]}